The present study focuses on the formulation and evaluation of a herbal powder shampoo using five medicinal herbs: Neem (Azadirachta indica), Tulsi (Ocimum tenuiflorum), Shikakai (Acacia concinna), Hibiscus (Rosa sinensis), and Brahmi (Bacopa monnieri). These herbs were selected for their scientifically validated hair care benefits, including antifungal, anti-inflammatory, and hair growth-promoting properties. The plant materials were collected, shade dried, powdered, sieved, and blended in appropriate proportions to form a fine dry shampoo. The formulation was evaluated through organoleptic properties, powder characteristics (particle size, angle of repose, bulk and tapped density), and physicochemical properties like pH, solubility, washability, dirt dispersion, and foaming ability. The final product exhibited a smooth and fine moss green powder with a pleasant herbal odor and favorable physicochemical characteristics. The shampoo showed good washability, high foaming index, no skin irritation, and remained stable at room temperature. The use of natural ingredients makes this herbal dry shampoo a safer alternative to chemicalbased shampoos. It offers a promising, eco-friendly, and effective hair care solution without harmful additives. This formulation can be further explored for commercial application, especially for consumers seeking natural, sustainable personal care options.